Two‐dimensional NMR spectra of sesquiterpenes. II—Noesy study of some sesquiterpene lactones with pseudoguaianolide, 3,4‐seco‐pseudoguaianolide and guaianolide skeletons

Ivana Aljančić‐Šolaja; Slobodan Milosavljević; Miodrag Djermanović; Milutin Stefanović; Slobodan Macura

doi:10.1002/mrc.1260260902

Two‐dimensional NMR spectra of sesquiterpenes. II—Noesy study of some sesquiterpene lactones with pseudoguaianolide, 3,4‐seco‐pseudoguaianolide and guaianolide skeletons

Ivana Aljančić‐Šolaja, Slobodan Milosavljević, Miodrag Djermanović, Milutin Stefanović, Slobodan Macura

Biochemistry and Molecular Biology

Research output: Contribution to journal › Article › peer-review

7 Scopus citations

Abstract

The application of phase‐sensitive 2D ¹H NOE NMR spectroscopy (PS NOESY) in the stereochemical assignment of sesquiterpene lactones such as 4‐oxo‐3,4‐seco‐ambrosan‐6,12‐olide‐3‐oic acid methyl ester, 4‐oxo‐6‐hydroxypseudoguai‐11(13)‐en‐8,12‐olide and 8‐angeloyloxy‐10‐acetoxyguai‐3‐en‐6‐,12‐olide is reported.

Original language	English (US)
Pages (from-to)	725-728
Number of pages	4
Journal	Magnetic Resonance in Chemistry
Volume	26
Issue number	9
DOIs	https://doi.org/10.1002/mrc.1260260902
State	Published - Sep 1988

Keywords

4‐Oxo‐3,4‐seco‐ambrosan‐6,12‐olide‐3‐oic acid methyl ester
4‐Oxo‐pseudoguai‐11(13)‐en‐8,12‐olide
8‐Angeloyloxy‐10‐acetoxyguai‐3‐en‐6,12‐olide
Phase‐sensitive NOESY
Sesquiterpene lactor es

ASJC Scopus subject areas

General Chemistry
General Materials Science

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10.1002/mrc.1260260902

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Two‐dimensional NMR spectra of sesquiterpenes. II—Noesy study of some sesquiterpene lactones with pseudoguaianolide, 3,4‐seco‐pseudoguaianolide and guaianolide skeletons. / Aljančić‐Šolaja, Ivana; Milosavljević, Slobodan; Djermanović, Miodrag et al.
In: Magnetic Resonance in Chemistry, Vol. 26, No. 9, 09.1988, p. 725-728.

Research output: Contribution to journal › Article › peer-review

Aljančić‐Šolaja, I, Milosavljević, S, Djermanović, M, Stefanović, M & Macura, S 1988, 'Two‐dimensional NMR spectra of sesquiterpenes. II—Noesy study of some sesquiterpene lactones with pseudoguaianolide, 3,4‐seco‐pseudoguaianolide and guaianolide skeletons', Magnetic Resonance in Chemistry, vol. 26, no. 9, pp. 725-728. https://doi.org/10.1002/mrc.1260260902

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title = "Two‐dimensional NMR spectra of sesquiterpenes. II—Noesy study of some sesquiterpene lactones with pseudoguaianolide, 3,4‐seco‐pseudoguaianolide and guaianolide skeletons",

abstract = "The application of phase‐sensitive 2D 1H NOE NMR spectroscopy (PS NOESY) in the stereochemical assignment of sesquiterpene lactones such as 4‐oxo‐3,4‐seco‐ambrosan‐6,12‐olide‐3‐oic acid methyl ester, 4‐oxo‐6‐hydroxypseudoguai‐11(13)‐en‐8,12‐olide and 8‐angeloyloxy‐10‐acetoxyguai‐3‐en‐6‐,12‐olide is reported.",

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author = "Ivana Aljan{\v c}i{\'c}‐{\v S}olaja and Slobodan Milosavljevi{\'c} and Miodrag Djermanovi{\'c} and Milutin Stefanovi{\'c} and Slobodan Macura",

year = "1988",

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doi = "10.1002/mrc.1260260902",

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AU - Aljančić‐Šolaja, Ivana

AU - Milosavljević, Slobodan

AU - Djermanović, Miodrag

AU - Stefanović, Milutin

AU - Macura, Slobodan

PY - 1988/9

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N2 - The application of phase‐sensitive 2D 1H NOE NMR spectroscopy (PS NOESY) in the stereochemical assignment of sesquiterpene lactones such as 4‐oxo‐3,4‐seco‐ambrosan‐6,12‐olide‐3‐oic acid methyl ester, 4‐oxo‐6‐hydroxypseudoguai‐11(13)‐en‐8,12‐olide and 8‐angeloyloxy‐10‐acetoxyguai‐3‐en‐6‐,12‐olide is reported.

AB - The application of phase‐sensitive 2D 1H NOE NMR spectroscopy (PS NOESY) in the stereochemical assignment of sesquiterpene lactones such as 4‐oxo‐3,4‐seco‐ambrosan‐6,12‐olide‐3‐oic acid methyl ester, 4‐oxo‐6‐hydroxypseudoguai‐11(13)‐en‐8,12‐olide and 8‐angeloyloxy‐10‐acetoxyguai‐3‐en‐6‐,12‐olide is reported.

KW - 4‐Oxo‐3,4‐seco‐ambrosan‐6,12‐olide‐3‐oic acid methyl ester

KW - 4‐Oxo‐pseudoguai‐11(13)‐en‐8,12‐olide

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KW - Phase‐sensitive NOESY

KW - Sesquiterpene lactor es

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Two‐dimensional NMR spectra of sesquiterpenes. II—Noesy study of some sesquiterpene lactones with pseudoguaianolide, 3,4‐seco‐pseudoguaianolide and guaianolide skeletons

Abstract

Keywords

ASJC Scopus subject areas

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