Two‐dimensional NMR spectra of sesquiterpenes. II—Noesy study of some sesquiterpene lactones with pseudoguaianolide, 3,4‐seco‐pseudoguaianolide and guaianolide skeletons

Ivana Aljančić‐Šolaja; Slobodan Milosavljević; Miodrag Djermanović; Milutin Stefanović; Slobodan I Macura

doi:10.1002/mrc.1260260902

Two‐dimensional NMR spectra of sesquiterpenes. II—Noesy study of some sesquiterpene lactones with pseudoguaianolide, 3,4‐seco‐pseudoguaianolide and guaianolide skeletons

Ivana Aljančić‐Šolaja, Slobodan Milosavljević, Miodrag Djermanović, Milutin Stefanović, Slobodan I Macura

Research output: Contribution to journal › Article › peer-review

7 Scopus citations

Abstract

The application of phase‐sensitive 2D ¹H NOE NMR spectroscopy (PS NOESY) in the stereochemical assignment of sesquiterpene lactones such as 4‐oxo‐3,4‐seco‐ambrosan‐6,12‐olide‐3‐oic acid methyl ester, 4‐oxo‐6‐hydroxypseudoguai‐11(13)‐en‐8,12‐olide and 8‐angeloyloxy‐10‐acetoxyguai‐3‐en‐6‐,12‐olide is reported.

Original language	English (US)
Pages (from-to)	725-728
Number of pages	4
Journal	Magnetic Resonance in Chemistry
Volume	26
Issue number	9
DOIs	https://doi.org/10.1002/mrc.1260260902
State	Published - 1988
Externally published	Yes

Keywords

4‐Oxo‐3,4‐seco‐ambrosan‐6,12‐olide‐3‐oic acid methyl ester
4‐Oxo‐pseudoguai‐11(13)‐en‐8,12‐olide
8‐Angeloyloxy‐10‐acetoxyguai‐3‐en‐6,12‐olide
Phase‐sensitive NOESY
Sesquiterpene lactor es

ASJC Scopus subject areas

Chemistry(all)
Materials Science(all)

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10.1002/mrc.1260260902

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Aljančić‐Šolaja, I., Milosavljević, S., Djermanović, M., Stefanović, M., & Macura, S. I. (1988). Two‐dimensional NMR spectra of sesquiterpenes. II—Noesy study of some sesquiterpene lactones with pseudoguaianolide, 3,4‐seco‐pseudoguaianolide and guaianolide skeletons. Magnetic Resonance in Chemistry, 26(9), 725-728. https://doi.org/10.1002/mrc.1260260902

Two‐dimensional NMR spectra of sesquiterpenes. II—Noesy study of some sesquiterpene lactones with pseudoguaianolide, 3,4‐seco‐pseudoguaianolide and guaianolide skeletons. / Aljančić‐Šolaja, Ivana; Milosavljević, Slobodan; Djermanović, Miodrag et al.

In: Magnetic Resonance in Chemistry, Vol. 26, No. 9, 1988, p. 725-728.

Research output: Contribution to journal › Article › peer-review

Aljančić‐Šolaja, I, Milosavljević, S, Djermanović, M, Stefanović, M & Macura, SI 1988, 'Two‐dimensional NMR spectra of sesquiterpenes. II—Noesy study of some sesquiterpene lactones with pseudoguaianolide, 3,4‐seco‐pseudoguaianolide and guaianolide skeletons', Magnetic Resonance in Chemistry, vol. 26, no. 9, pp. 725-728. https://doi.org/10.1002/mrc.1260260902

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abstract = "The application of phase‐sensitive 2D 1H NOE NMR spectroscopy (PS NOESY) in the stereochemical assignment of sesquiterpene lactones such as 4‐oxo‐3,4‐seco‐ambrosan‐6,12‐olide‐3‐oic acid methyl ester, 4‐oxo‐6‐hydroxypseudoguai‐11(13)‐en‐8,12‐olide and 8‐angeloyloxy‐10‐acetoxyguai‐3‐en‐6‐,12‐olide is reported.",

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author = "Ivana Aljan{\v c}i{\'c}‐{\v S}olaja and Slobodan Milosavljevi{\'c} and Miodrag Djermanovi{\'c} and Milutin Stefanovi{\'c} and Macura, {Slobodan I}",

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doi = "10.1002/mrc.1260260902",

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AU - Aljančić‐Šolaja, Ivana

AU - Milosavljević, Slobodan

AU - Djermanović, Miodrag

AU - Stefanović, Milutin

AU - Macura, Slobodan I

PY - 1988

Y1 - 1988

N2 - The application of phase‐sensitive 2D 1H NOE NMR spectroscopy (PS NOESY) in the stereochemical assignment of sesquiterpene lactones such as 4‐oxo‐3,4‐seco‐ambrosan‐6,12‐olide‐3‐oic acid methyl ester, 4‐oxo‐6‐hydroxypseudoguai‐11(13)‐en‐8,12‐olide and 8‐angeloyloxy‐10‐acetoxyguai‐3‐en‐6‐,12‐olide is reported.

AB - The application of phase‐sensitive 2D 1H NOE NMR spectroscopy (PS NOESY) in the stereochemical assignment of sesquiterpene lactones such as 4‐oxo‐3,4‐seco‐ambrosan‐6,12‐olide‐3‐oic acid methyl ester, 4‐oxo‐6‐hydroxypseudoguai‐11(13)‐en‐8,12‐olide and 8‐angeloyloxy‐10‐acetoxyguai‐3‐en‐6‐,12‐olide is reported.

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KW - 4‐Oxo‐pseudoguai‐11(13)‐en‐8,12‐olide

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KW - Phase‐sensitive NOESY

KW - Sesquiterpene lactor es

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Two‐dimensional NMR spectra of sesquiterpenes. II—Noesy study of some sesquiterpene lactones with pseudoguaianolide, 3,4‐seco‐pseudoguaianolide and guaianolide skeletons

Abstract

Keywords

ASJC Scopus subject areas

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